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The final product (698 mg) was obtained in 54% yield and characterized by the analytic reversed-phase HPLC and 1 H NMR with a JEOL JNX-ECX500 spectrometer (Tokyo, Japan)
Step 6: Slowly depress the plunger until all the solution is injected, then withdraw the needle smoothly
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Three patients discontinued treatment due to adverse events, with one patient each from the placebo, 12 mg, and 15 mg-1 groups
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