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The synthesis initiated with the direct chlorination of Compound 35 , yielding chloroindane methyl ester 36 , which, after chiral resolution using HPLC, afforded Compound 32 (Scheme 5) (Humphrey, 2014)
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Differences in trial duration, drug exposure, target engagement and outcome sensitivityall may have factored in
Then, the mixture was incubated for 5 h at 4 C
95% CI, 1.21 to 2.67) [35]
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