Metoclopramide Hydrochloride Monohydrate USP size:25 KG 5 WATER DETERMINATION 3

5 WATER DETERMINATION 3

Test Specification Min Max FDA LOT NUMBER EXPIRATION DATE

50% COLOR (APHA) 10 ECD RESPONSIVE RESIDUE (as[nHEPTACHLOR EPOXIDE) 10 ppt FID RESPONSIVE RESIDUE (as 2-OCTANOL) 5 ppb RESIDUE AFTER EVAPORATION 1 ppm WATER 0

Test Specification Min Max ODOR ODORLESS ODORLESS ASSAY (H[@3@]BO[@3@]

1M SOLUTION @ 25[dC 9

Metoclopramide Hydrochloride Monohydrate USP size:25 KG 5 WATER DETERMINATION 3Test Specification Min Max ASSAY (ANHYDROUS BASIS) 98 101. 00% WATER DETERMINATION 4. 5 6. 00% RESIDUE ON IGNITION 0. 10% ORGANIC IMPURITIES: N ACETYLMETOCLOPRAMIDE ( METOCLOPRAMIDE RELATED CPD. A ) 0. 15% METHYL 4 ACETAMIDO 2 METHOXYBENZOATE ( METOCLOPRAMIDE RELATED COMPOUND D) 0. 15% N ACETYL METHYL ESTER ANALOG (METOLOPRAMIDE RELATED COMPOUND B) 0. 15% ANY OTHER INDIVIDUAL IMPURITY 0. 10% TOTAL IMPURITIES 0. 50% ELEMENTAL IMPURITIES AS REPORTED AS